The present study was aimed to evaluate physicochemical standardization and preliminary phytochemical investigation of the leaf of Grewia tiliaefolia Vahl belonging to the family tiliaceae. The standardization parameters included determination of foreign matter, loss on drying, ash values, extractive values, fluorescence analysis, preliminary phytochemical screening was performed according to standard procedures. The preliminary identification was done by using Macroscopical observation and final authenticity was done by botanist.