The electrochemical behavior of Fexinidazole is studied by employing Cyclic Voltammetry (CV) and Differential Pulse Polarography (DPP) in universal buffers of PH ranging from 2.0 to 12.0. The kinetic parameters such as transfer co-efficient, diffusion co-efficients, and heterogeneous forward rate constant values are evaluated by employing these techniques. Differential Pulse Polarography is employed for the estimation of Fexinidazole in selected pharmaceutical formulations.